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George MacLeod:
MPhil (University of Bournemouth) BSc (Robert Gordon's University Aberdeen) Chief Technician
Department of Environmental Science University of Stirling
Stirling FK9 4LA, Scotland.
Office +44(0)1789-467856 Lab +44(0)1786467858
e-mail g.w.macleod@stir.ac.uk
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Current
Position:
Current
Duties:
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Chief
Technician for Micromorphology and thin section labs.
Production of soil thin section slides for both research
and consultancy
Operation
& maintenance of microscopes and AnalySIS
image analysis system.
Operation of the GF-AAS system.
Design and maintenance of the micromorphology web site.
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Experience:
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I
have a number of years experience as an analytical chemist
using both wet chemistry and instrumental techniques.
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IC
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I have used ion chromatography extensively over the
years for a variety of analysis, ranging from amino
acids in soil extracts (which I used for my MPhil
Thesis)to efflorescent salts in mortar samples from
Windsor Castle amongst others.
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GF-AAS
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The technique of Atomic Absorption is used to quantify
metal elements in solutions. Examples of use: Cd in
industrial discharge, Pb in human hair, Cd in aphids,
Mg, K, Ca, Al, Fe, Mn, Ni, Cu etc. in soils and ground
waters.
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FTIR
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used
to identify particular molecular bonds by absorbtion of
infra-red radiation, examples of use are the identification
of blood in mortar samples and the identification of wax
on an Egyptian mummy as contemporary.
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HPLC
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A
very versatile chromatography technique used to seperate
components in the liquid phase.
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GC
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Another chromatography technique used
to seperate components in the gas phase.
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SEM/EDX
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instrument uses a beam of electrons to produce high resolution
images and by analysisng the x-rays given off by samples
and elemental analysis can be performed. I have used this
technique over a wide range of applications from stress
fractures in aircraft fuel systems to elemental analysis
of ancient pottery.
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UV-VIS
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spectrophotometry technique, this time using electro magnetic
radiation in the ultra violet and visible regions. Exaples
of use are the analysis of medieval glass and determination
of phosphate in soil by ammonium molybdate method.
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